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Table B13. Recovery (percent) of PCB, pesticide, and PAH surrogate internal standards in bluefish muscle composites

Composite #
PCBs and Pesticides
PAHsa
4,4'-
dibromoocta-
fluorobiphenyl
BZ #198 1,2,3-trichloro-
benzene
Ronnel Naph-
thalene
Acenaph-
thylene
Chrysene Pyrene

Benzo[ghi]-
perylene

Station BL1
101 80 95 81 136 27 48 134 97 90
102 67 89 65 93 17 50 104 104 139
103 59 90 84 85 33 50 158 84 10
104 69 90 70 73 27 46 111 91 50
105 64 94 115 107 23 46 61 82 22
Station BL2
106 62 102 61 81 25 53 120 100 13
107 72 95 154 81 16 44 101 102 18
107-dup. 75 96 164 86 23 50 115 102 31
107-trip. 72 101 84 87 29 59 95 101 16
107 mean (n = 3) 73 97 134 85 23 51 104 102 21
108 68 99 102 84 28 53 75 98 8
109 58 90 74 73 37 57 117 97 11
110 66 83 81 88 32 47 79 77 0

Station BL3

111 77 84 460 87 34 56 146 103 15
112 69 95 108 72 55 67 188 104 26
113 87 69 564 85 32 53 66 68 9
114 78 91 337 101 54 61 132 115 0
 
Mean (n = 14) 70 91 167 89 32 53 114 95 30
Std. dev. 8 8 157 16 11 6 35 12 38

aAll aromatic hydrogen atoms labeled with deuterium [2H] atoms: naphthalene and acenaphthylene with 8 x [2H], pyrene with 10 x [2H], and chyrsene and benzo[ghi]perylene with 12 x [2H].

Table B14

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(File Modified Nov. 19 2010)